LCMS data
Crude drug latin name | PINELLIAE TUBER | |||||||
Sample | NIB-0334 | |||||||
CHROM_NAME | ESI-Orbitrap(+) | |||||||
CHROM_TYPE | LC | |||||||
LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |||||||
MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |||||||
Column | FILTER | ODS | ||||||
LENGTH | 100mm | |||||||
DIAMETER | 2.1mm | |||||||
PARTICLES_SIZE | 2.2 μm | |||||||
MANUFACTURER | Thermo Fisher Scientific | |||||||
PRODUCT_NAME | Acclaim RSLC 120 C18 | |||||||
LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile | ||||||
LC_G_PROGRAM | B = 2% - 60 % (40 min) - 100 % (50 min) | |||||||
COLUMN_TEMP | 40℃ | |||||||
FLOW_RATE | 0.2 mL/min | |||||||
MS Measurement condition | Ionization mode | positive | ||||||
Desolvationtemperature | 275℃ | |||||||
Needle voltage | 3000V | |||||||
Velocity of Spectrum | 10 spec./sec. | |||||||
Range of m/z | 100-2000 | |||||||
Collision gas | He | |||||||
TIC_JCAMP_FILE | NIB-0334(+).jdx | |||||||
3D(PDA) data | ||||||||
UV data | ||||||||
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MEMO | sample: HANGE (Pinellia Tuber) water ext. 4 mg/mL (water/methanol 1:1) Injection Volume: 20μL ハンゲ 水抽出エキス 4 mg/mL 注入量: 20μL | |||||||
MS data list |