Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameALISMATIS RHIZOMA
SampleNIB-0369
CHROM_NAMEESI-Orbitrap(-)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific, Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific, LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE2.2μm
MANUFACTURERThermoScientific
PRODUCT_NAMEAcclaim RSLC 120 C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5% (0 min) - 70 % (30 min) - 100 % (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature275 ℃
Needle voltage-3000V
Velocity of Spectrum10 spectrum/sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0369(-).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 - 400
Memomeasured on a PDA
MEMOsample: TAKUSHA (Alisma Tuber) water ext. 4 mg/mL (water/methanol = 1:1)
Injection Volume: 20 μL

タクシャ 水抽出エキス 4 mg/mL(水/メタノール 1:1 溶液)
注入量:20 μL
MS data list
Compound dataRetention time(min)MS data
Alisol B Acetate(酢酸アリソールB) MS data