Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameSINOMENI CAULIS ET RHIZOMA
SampleNIB-0588
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEShimadzu UFLC
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap XL
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE1.9 μm
MANUFACTURERThermo Fisher Scientific
PRODUCT_NAMEHypersil GOLD
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 2% - 30 % (20 min) - 100 % (30 min) - 100 % (35 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature300℃
Needle voltage4000V
Velocity of Spectrum
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0588(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 - 800
Memomeasured on a PDA
MEMOsample: BOUI (Sinomenium Stem and Rhizome) water ext. 1 mg/mL (water/methanol 1:1)
Injection Volume: 10μL

ボウイ 水抽出エキス 1 mg/mL
注入量: 10μL
MS data list
Compound dataRetention time(min)MS data
Magnoflorine(マグノフロリン) 12.17 MS data
Sinomenine(シノメニン) 10.25 MS data