LCMS data
Crude drug latin name | ANEMARRHENAE RHIZOMA | |
Sample | NIB-0526 | |
CHROM_NAME | ESI-Orbitrap(-) | |
CHROM_TYPE | LC | |
LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |
MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |
Column | FILTER | ODS |
LENGTH | 100mm | |
DIAMETER | 2.1mm | |
PARTICLES_SIZE | 2.6 μm | |
MANUFACTURER | ChromaNik Technologies | |
PRODUCT_NAME | SunShell C18 | |
LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile |
LC_G_PROGRAM | B = 2% - 70 % (15 min) - 100 % (16 min) - 100 % (17 min) | |
COLUMN_TEMP | 40℃ | |
FLOW_RATE | 0.5 mL/min | |
MS Measurement condition | Ionization mode | negative |
Desolvationtemperature | 275℃ | |
Needle voltage | 3000V | |
Velocity of Spectrum | 10 spec./sec. | |
Range of m/z | 100-2000 | |
Collision gas | He | |
TIC_JCAMP_FILE | NIB-0526(-).jdx | |
3D(PDA) data | ||
UV data | ||
MEMO | sample: CHIMO (Anemarrhena Rhizome) water ext. 1 mg/mL (water/methanol 1:1) Injection Volume: 10μL チモ 水抽出エキス 1 mg/mL (水/メタノール 1:1溶液) 注入量: 10μL | |
MS data list |