Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin namePHELLODENDRI CORTEX
SampleNIB-0655
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERChromaNik Technologies
PRODUCT_NAMESunShell C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 2% - 100 % (15 min) - 100 % (17 min)
COLUMN_TEMP40℃
FLOW_RATE0.3 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature275℃
Needle voltage3000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0655(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: OUBAKU (Phellodendron Bark) water ext.
pos 100 µg/mL , neg 500 µg/mL (water/methanol 1:1)
Injection Volume: 3µL

オウバク 水抽出エキス
正イオン検出100 μg/mL、負イオン検出500 μg/mL (水/メタノール 1:1溶液) に調製
注入量: 3μL
MS data list
Compound dataRetention time(min)MS data
Berberine (ベルベリン) 7.49 MS data
Jateorrhizine (ジャトロリジン) 6.92 MS data
Magnoflorine(マグノフロリン) 4.99 MS data
Phellodendrine (フェロデンドリン) 4.75 MS data