LCMS data
| Crude drug latin name | DIOSCOREAE RHIZOMA | |||||||
| Sample | NIB-0748 | |||||||
| CHROM_NAME | ESI-Orbitrap(-) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 100mm | |||||||
| DIAMETER | 2.1mm | |||||||
| PARTICLES_SIZE | 2.6 μm | |||||||
| MANUFACTURER | ChromaNik Technologies | |||||||
| PRODUCT_NAME | SunShell C18 | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile | ||||||
| LC_G_PROGRAM | B = 2% - 70 % (15 min) - 100 % (16 min) - 100 % (17 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.25 mL/min | |||||||
| MS Measurement condition | Ionization mode | negative | ||||||
| Desolvationtemperature | 275℃ | |||||||
| Needle voltage | -3000V | |||||||
| Velocity of Spectrum | 10 spec./sec. | |||||||
| Range of m/z | 100-2000 | |||||||
| Collision gas | He | |||||||
| TIC_JCAMP_FILE |  NIB-0748(-).jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
| ||||||||
| MEMO | sample: SAN-YAKU (Dioscorea Rhizome) water ext. 2mg/mL (water/methanol 1:1) Injection Volume: pos 10µL, neg 15µL サンヤク 水抽出エキス 2mg/mL （水/メタノール 1:1溶液） 注入量： pos 10μL、neg 15μL | |||||||
| MS data list | ||||||||
