Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameCORNI FRUCTUS
SampleNIB-0648
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERChromaNik Technologies
PRODUCT_NAMESunShell C18
LC Measurement conditionMOBILE_PHASEA = 10mM ammonium formate in ultrapure water; B = 0.01% formic acid in acetonitrile
LC_G_PROGRAMB = 1% - 1 % (1 min) - 40 % (12 min) - 100 % (14 min) - 100 % (16 min)
COLUMN_TEMP40℃
FLOW_RATE0.3 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature275℃
Needle voltage3000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0648(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample:SANSHUYU (Cornus Fruit) water ext.
1mg/mL (water/methanol 1:1)
Injection Volume: 5µL

サンシュユ 水抽出エキス 1mg/mL (水/メタノール 1:1溶液)
注入量: 5μL
MS data list
Compound dataRetention time(min)MS data
Morroniside (モロニシド) 5.94 MS data
Loganin(ロガニン) 6.86 MS data