LCMS data
Crude drug latin name | CLEMATIDIS RADIX | |||||||
Sample | NIB-1126 | |||||||
CHROM_NAME | ESI-Orbitrap(+) | |||||||
CHROM_TYPE | LC | |||||||
LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |||||||
MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |||||||
Column | FILTER | ODS | ||||||
LENGTH | 100mm | |||||||
DIAMETER | 2.1mm | |||||||
PARTICLES_SIZE | 2.6 μm | |||||||
MANUFACTURER | ChromaNik Technologies | |||||||
PRODUCT_NAME | SunShell C18 | |||||||
LC Measurement condition | MOBILE_PHASE | A = 10mM ammonium formate in ultrapure water; B = 10mM ammonium formate in MeOH : EtOH : acetonitrile = 1 : 2 : 7 | ||||||
LC_G_PROGRAM | B = 1% - 1 % (1 min) - 50 % (10 min) - 100 % (16 min) - 100 % (17 min) | |||||||
COLUMN_TEMP | 40℃ | |||||||
FLOW_RATE | 0.3 mL/min | |||||||
MS Measurement condition | Ionization mode | positive | ||||||
Desolvationtemperature | 250℃ | |||||||
Needle voltage | 3000V | |||||||
Velocity of Spectrum | 10 spec./sec. | |||||||
Range of m/z | 100-2000 | |||||||
Collision gas | He | |||||||
TIC_JCAMP_FILE | NIB-1126(+).jdx | |||||||
3D(PDA) data | ||||||||
UV data | ||||||||
| ||||||||
MEMO | sample: IREISEN (Clematis Root) water ext. 1mg/mL (water/methanol 1:1) Injection Volume: pos. 5µL neg. 10µL イレイセン 水抽出エキス 1mg/mL (水/メタノール 1:1溶液) 注入量: 正イオン検出5μL 、 負イオン検出 10μL | |||||||
MS data list |