Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameCLEMATIDIS RADIX
SampleNIB-1126
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERChromaNik Technologies
PRODUCT_NAMESunShell C18
LC Measurement conditionMOBILE_PHASEA = 10mM ammonium formate in ultrapure water; B = 10mM ammonium formate in MeOH : EtOH : acetonitrile = 1 : 2 : 7
LC_G_PROGRAMB = 1% - 1 % (1 min) - 50 % (10 min) - 100 % (16 min) - 100 % (17 min)
COLUMN_TEMP40℃
FLOW_RATE0.3 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature250℃
Needle voltage3000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-1126(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: IREISEN (Clematis Root) water ext. 1mg/mL (water/methanol 1:1)
Injection Volume: pos. 5µL neg. 10µL

イレイセン 水抽出エキス 1mg/mL (水/メタノール 1:1溶液)
注入量: 正イオン検出5μL 、 負イオン検出 10μL
MS data list