Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameCORYDALIS TUBER
SampleNIB-0988
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERChromaNik Technologies
PRODUCT_NAMESunShell C18
LC Measurement conditionMOBILE_PHASEA = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile
LC_G_PROGRAMB = 1% - 1 % (0.5 min) - 5 % (1 min) - 35 % (13 min) - 100 % (15 min) – 100 % (16 min)
COLUMN_TEMP40℃
FLOW_RATE0.3 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature275℃
Needle voltage+3000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0988(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: ENGOSAKU (Corydalis Tuber) water ext. 0.1mg/mL (water/methanol 1:1)
Injection Volume: 15µL

エンゴサク 水抽出エキス 0.1mg/mL (水/メタノール 1:1溶液)
注入量: 15μL
MS data list
Compound dataRetention time(min)MS data
Glaucine (グラウシン) 8.63 MS data
Dehydrocorydaline (デヒドロコリダリン) 10.35 MS data
Corydaline (コリダリン) 9.33 MS data