LCMS data
| Crude drug latin name | ZINGIBERIS PROCESSUM RHIZOMA | |||||||
| Sample | NIB-0796 | |||||||
| CHROM_NAME | APCI-Orbitrap(-) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 100 mm | |||||||
| DIAMETER | 2.1mm | |||||||
| PARTICLES_SIZE | 1.9 um | |||||||
| MANUFACTURER | Thermo Scientific | |||||||
| PRODUCT_NAME | Hypersil GOLD C18 | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile | ||||||
| LC_G_PROGRAM | B = 1 % (0 min) - 1 % (1 min) - 60 % (8 min) – 100 % (10 min) - 100 % (12 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.4 mL/min | |||||||
| MS Measurement condition | Ionization mode | negative | ||||||
| Desolvationtemperature | 400 ℃ | |||||||
| Needle voltage | 6000 V | |||||||
| Velocity of Spectrum | 10 spec./sec. | |||||||
| Range of m/z | 100-2000 | |||||||
| Collision gas | He | |||||||
| TIC_JCAMP_FILE |  NIB-0796(-).jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
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| MEMO | sample: KANKYOU (Processed Ginger) water ext. 2 mg/mL (methanol:water = 1:1) Injection Volume: 5 μL カンキョウ 水抽出エキス 2 mg/mL (メタノール:水 1:1 溶液) 注入量： 5 μL | |||||||
| MS data list | ||||||||
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