LCMS data
| Crude drug latin name | CHRYSANTHEMI FLOS | |||||||
| Sample | NIB-0804 | |||||||
| CHROM_NAME | ESI-Orbitrap(+) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 50mm | |||||||
| DIAMETER | 2.1mm | |||||||
| PARTICLES_SIZE | 1.7μm | |||||||
| MANUFACTURER | Phenomenex | |||||||
| PRODUCT_NAME | Kinetex C18 | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile | ||||||
| LC_G_PROGRAM | B = 20% - 20 % (1 min) - 60 % (6 min) - 95 % (11 min) - 95 % (13 min) | |||||||
| COLUMN_TEMP | 30℃ | |||||||
| FLOW_RATE | 0.2 mL/min | |||||||
| MS Measurement condition | Ionization mode | positive | ||||||
| Desolvationtemperature | 0℃ | |||||||
| Needle voltage | 4000V | |||||||
| Velocity of Spectrum | 10 spec./sec. | |||||||
| Range of m/z | 150-2000 | |||||||
| Collision gas | He | |||||||
| TIC_JCAMP_FILE |  NIB-0804(+).jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
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| MEMO | sample: KIKUKA (Chrysanthemum Flower) water ext. 1mg/mL (water/methanol 1:1) Injection Volume: pos 2µL, neg 1µL キクカ 水抽出エキス 1mg/mL （水/メタノール 1:1溶液） 注入量： 正イオン検出：2μL、負イオン検出：1μL | |||||||
| MS data list | ||||||||
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