Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameCHRYSANTHEMI FLOS
SampleNIB-0810
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH50mm
DIAMETER2.1mm
PARTICLES_SIZE1.7μm
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile
LC_G_PROGRAMB = 20% - 20 % (1 min) - 60 % (6 min) - 95 % (11 min) - 95 % (13 min)
COLUMN_TEMP30℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature0℃
Needle voltage4000V
Velocity of Spectrum10 spec./sec.
Range of m/z150-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0810(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: KIKUKA (Chrysanthemum Flower) water ext.
1mg/mL (water/methanol 1:1)
Injection Volume: pos 2µL, neg 1µL

キクカ 水抽出エキス
1mg/mL (水/メタノール 1:1溶液)
注入量: 正イオン検出:2μL、負イオン検出:1μL
MS data list
Compound dataRetention time(min)MS data
Linarin (リナリン) 5.52 MS data