Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin namePOLYGALAE RADIX
SampleNIB-0260
CHROM_NAMEESI-Orbitrap(-)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERChromaNik Technologies
PRODUCT_NAMESunShell
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) Formic acid in ultrapure water; B = 0.1% (v/v) Formic acid in acetonitrile
LC_G_PROGRAMB = 2%(0 min) - 100 % (15 min) - 100 % (18 min)
COLUMN_TEMP40℃
FLOW_RATE0.25 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature275℃
Needle voltage3000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0260(-).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 - 400
Memomeasured on a PDA
MEMOsample: ONJI (Polygala Root) water ext. 1 mg/mL (water/methanol 1:1)
Injection Volume: 10μL

オンジ 水抽出エキス 1 mg/mL(水:メタノール 1:1溶液)
注入量: 10μL
MS data list