Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameMAGNOLIAE CORTEX
SampleNIB-0686
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEShimadzu UFLC
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap XL
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE1.9 μm
MANUFACTURERThermo Fisher Scientific
PRODUCT_NAMEHypersil GOLD
LC Measurement conditionMOBILE_PHASEA = 10mM ammonium acetate in ultrapure water; B = 10mM ammonium acetate in acetonitrile
LC_G_PROGRAMB = 5% - 50 % (14 min) - 100 % (18 min) - 100 % (20 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature300℃
Needle voltage4000V
Velocity of Spectrum
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0686(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 - 800
Memomeasured on a PDA
MEMOsample: KOUBOKU (Magnolia Bark) water ext. 1 mg/mL (water/methanol 1:1)
Injection Volume: pos 4μL , neg 5μL

コウボク 水抽出エキス 1 mg/mL (水/メタノール 1:1溶液)
注入量: ボジティブモード 4μL, ネガティブモード 5μL
MS data list