LCMS data
| Crude drug latin name | MAGNOLIAE CORTEX | |||||||
| Sample | NIB-0686 | |||||||
| CHROM_NAME | ESI-Orbitrap(-) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | Shimadzu UFLC | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap XL | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 100mm | |||||||
| DIAMETER | 2.1mm | |||||||
| PARTICLES_SIZE | 1.9 μm | |||||||
| MANUFACTURER | Thermo Fisher Scientific | |||||||
| PRODUCT_NAME | Hypersil GOLD | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 10mM ammonium acetate in ultrapure water; B = 10mM ammonium acetate in acetonitrile | ||||||
| LC_G_PROGRAM | B = 5% - 50 % (14 min) - 100 % (18 min) - 100 % (20 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.2 mL/min | |||||||
| MS Measurement condition | Ionization mode | negative | ||||||
| Desolvationtemperature | 300℃ | |||||||
| Needle voltage | 4000V | |||||||
| Velocity of Spectrum | ||||||||
| Range of m/z | 100-2000 | |||||||
| Collision gas | He | |||||||
| TIC_JCAMP_FILE |  NIB-0686(-).jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
| ||||||||
| MEMO | sample: KOUBOKU (Magnolia Bark) water ext. 1 mg/mL (water/methanol 1:1) Injection Volume: pos 4μL , neg 5μL コウボク 水抽出エキス 1 mg/mL （水/メタノール 1:1溶液） 注入量： ボジティブモード 4μL, ネガティブモード 5μL | |||||||
| MS data list | ||||||||
