Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameGARDENIAE FRUCTUS
SampleNIB-0019
CHROM_NAMEESI-Q-TOF(-)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH150mm
DIAMETER2.0mm
PARTICLES_SIZE3μm
MANUFACTURERKANTO CHEMICAL
PRODUCT_NAMEMightysil ODS
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 0 - 70 % (30 min) – 100 % (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature450 ℃
Needle voltage-3,500 V
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0019(-).jdx
3D(PDA) data
UV data
MEMOsample: SANSHISHI (Gardenia Fruit) water ext. 0.5 mg/mL(water/methanol)
Injection Volume: 5 μL

サンシシ 水抽出エキス 0.5mg/mL(水/メタノール溶液)
注入量:5 μL
MS data list
Compound dataRetention time(min)MS data
Geniposide(ゲニポシド) 15.308 MS data