Crude drug latin name | LITHOSPERMI RADIX |
Sample | NIB-0852 |
CHROM_NAME | ESI-Orbitrap(+) |
CHROM_TYPE | LC |
LC MACHINE TYPE | Shimadzu 30A |
MS MACHINE TYPE | ThermoFisher Scientific Orbitrap Velos Pro |
Column | FILTER | ODS |
LENGTH | 150mm |
DIAMETER | 2.0 mm |
PARTICLES_SIZE | 5 µm |
MANUFACTURER | Nomura Chemical |
PRODUCT_NAME | Develosil C30-UG |
LC Measurement condition | MOBILE_PHASE | A = 10mM ammonium formate in ultrapure water; B = acetonitrile |
LC_G_PROGRAM | B = 2% - 2 % (5 min) - 95 % (18 min) - 95 % (25 min) |
COLUMN_TEMP | 40℃ |
FLOW_RATE | 0.3 mL/min |
MS Measurement condition | Ionization mode | positive |
Desolvationtemperature | 450 ℃ |
Needle voltage | 3000V |
Velocity of Spectrum | |
Range of m/z | 100-2000 |
Collision gas | N2 |
TIC_JCAMP_FILE | NIB-0852(+).jdx |
3D(PDA) data | |
UV data |
UV chromatogram | |
Wavelength(nm) | 190 - 400 |
Memo | measured on a PDA |
|
MEMO | sample: SHIKON (Lithospermum Root) water ext.
Injection Volume: 10 μL |
MS data list |
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