Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameLITHOSPERMI RADIX
SampleNIB-0900
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEShimadzu 30A
MS MACHINE TYPEThermoFisher Scientific Orbitrap Velos Pro
ColumnFILTERODS
LENGTH150mm
DIAMETER2.0 mm
PARTICLES_SIZE5 µm
MANUFACTURERNomura Chemical
PRODUCT_NAMEDevelosil C30-UG
LC Measurement conditionMOBILE_PHASEA = 10mM ammonium formate in ultrapure water; B = acetonitrile
LC_G_PROGRAMB = 2% - 2 % (5 min) - 95 % (18 min) - 95 % (25 min)
COLUMN_TEMP40℃
FLOW_RATE0.3 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature450 ℃
Needle voltage3000V
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2
TIC_JCAMP_FILE
NIB-0900(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 - 400
Memomeasured on a PDA
MEMOsample: SHIKON (Lithospermum Root) water ext.
Injection Volume: 10 μL
MS data list
Compound dataRetention time(min)MS data
lithosenine (リトセニン) 10.27 MS data
acetyllithosenine (アセチルリトセニン) 11.01 MS data