LCMS data
| Crude drug latin name | ANGELICAE DAHURICAE RADIX | |||||||
| Sample | NIB-1033 | |||||||
| CHROM_NAME | ESI-Orbitrap(-) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | Shimadzu 30A | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific Orbitrap Velos Pro | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 150mm | |||||||
| DIAMETER | 2.0 mm | |||||||
| PARTICLES_SIZE | 3 µm | |||||||
| MANUFACTURER | YMC | |||||||
| PRODUCT_NAME | YMC-Triart C18 | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 0.1% formic acid in ultrapure water; B = acetonitrile | ||||||
| LC_G_PROGRAM | B = 5% - 5 % (2 min) - 95 % (18 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.3 mL/min | |||||||
| MS Measurement condition | Ionization mode | negative | ||||||
| Desolvationtemperature | 450 ℃ | |||||||
| Needle voltage | 2500V | |||||||
| Velocity of Spectrum | ||||||||
| Range of m/z | 100-2000 | |||||||
| Collision gas | N2 | |||||||
| TIC_JCAMP_FILE |  NIB-1033(-).jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
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| MEMO | sample: BYAKUSHI (Angelica Dahurica Root) water ext. Injection Volume: 10 μL | |||||||
| MS data list | ||||||||
