LCMS data
| Crude drug latin name | GENTIANAE SCABRAE RADIX | |||||||
| Sample | NIB-1090 | |||||||
| CHROM_NAME | ESI-Orbitrap(+) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 150mm | |||||||
| DIAMETER | 2.1mm | |||||||
| PARTICLES_SIZE | 2.6 μm | |||||||
| MANUFACTURER | Phenomenex | |||||||
| PRODUCT_NAME | Kinetex C18 | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile | ||||||
| LC_G_PROGRAM | B = 2% - 2 % (2 min) - 40% (10 min.) - 98 % (15 min) - 98 % (18 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.2 mL/min | |||||||
| MS Measurement condition | Ionization mode | positive | ||||||
| Desolvationtemperature | 230℃ | |||||||
| Needle voltage | 3000V | |||||||
| Velocity of Spectrum | 10 spec./sec. | |||||||
| Range of m/z | 100-2000 | |||||||
| Collision gas | He | |||||||
| TIC_JCAMP_FILE |  NIB-1090(+).jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
| ||||||||
| MEMO | sample: RYUUTAN (Japanese Gentian) water ext. 5mg/mL (water/methanol 1:1) Injection Volume: 3μL リュウタン 水抽出エキス 5 mg/mL （水/メタノール 1:1溶液） 注入量： 3μL | |||||||
| MS data list | ||||||||
| ||||||||
