Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameARALIAE CORDATAE RHIZOMA
SampleNIB-1000
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH150mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile
LC_G_PROGRAMB = 2% - 2 % (2 min) - 98 % (40 min) - 98 % (45 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature230℃
Needle voltage3000V
Velocity of Spectrum10 spec./sec.
Range of m/z120-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-1000(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190-400
Memomeasured on a PDA
MEMOsample: DOKUKATSU (Aralia Rhizome) water ext. 2 mg/mL (water/methanol 1:1)
Injection Volume: 5μL

ドクカツ 水抽出エキス 2 mg/mL (水/メタノール 1:1溶液)
注入量: 5μL
MS data list
Compound dataRetention time(min)MS data
Chlorogenic acid (クロロゲン酸) 10.12 MS data