Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameZIZYPHI SEMEN
SampleNIB-0876
CHROM_NAMEESI-Orbitrap(-)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH150mm
DIAMETER2 mm
PARTICLES_SIZE3μm
MANUFACTURERImtakt
PRODUCT_NAMECadenza CD-C18
LC Measurement conditionMOBILE_PHASEA = 10mM ammonium formate in ultrapure water; B = 0.1% formic acid in acetonitrile
LC_G_PROGRAMB = 10% - 10 % (2 min) - 40 % (15 min) - 98 % (20 min) - 98 % (27 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature230℃
Needle voltage3000V
Velocity of Spectrum10 spec./sec.
Range of m/z155-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0876(-).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190-400
Memomeasured on a PDA
MEMOsample: SANSOUNIN (Jujube Seed) water ext. 4 mg/mL (water/methanol 1:1)
Injection Volume: 5μL

サンソウニン 水抽出エキス 4 mg/mL (水/メタノール 1:1溶液)
注入量: 5μL
MS data list