Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameSAUSSUREAE RADIX
SampleNIB-1066
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH150mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile
LC_G_PROGRAMB = 2% - 2 % (2 min) - 60 % (8 min) - 98 % (17 min) -98 % (20 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature270℃
Needle voltage4000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-1066(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190-400
Memomeasured on a PDA
MEMOsample: MOKKOU (Saussurea Root) water ext. 2 mg/mL (water/methanol 1:1)
Injection Volume: 5μL

モッコウ 水抽出エキス 2 mg/mL (水/メタノール 1:1溶液)
注入量: 5μL
MS data list
Compound dataRetention time(min)MS data
Dehydrocostuslactone(デヒドロコスツスラクトン) 12.81 MS data
Costunolide (コスツノリド) 12.59 MS data