Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameGLYCYRRHIZAE RADIX PRAEPARATA
SampleNIB-1185
CHROM_NAMEESI-Orbitrap(-)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH150mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile
LC_G_PROGRAMB = 10% - 10 % (2 min) - 50 % (14 min) - 98 % (17 min) - 98 % (21 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature270℃
Needle voltage4000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-1185(-).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190-400
Memomeasured on a PDA
MEMOsample: SHAKANZOU (Prepared Glycyrrhiza) water ext. 2 mg/mL (water/methanol 1:1)
Injection Volume: 1μL

シャカンゾウ水抽出エキス 2 mg/mL (水/メタノール 1:1溶液)
注入量: 1μL
MS data list
Compound dataRetention time(min)MS data
Glycyrrhizin(グリチルリチン) 15.53 MS data
Liquiritin(リクイリチン) 9.05 MS data