LCMS data
| Crude drug latin name | ELEUTHEROCOCCI SENTICOSI RHIZOMA | |||||||
| Sample | NIB-1178 | |||||||
| CHROM_NAME | ESI-Orbitrap(-) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 150 mm | |||||||
| DIAMETER | 2 mm | |||||||
| PARTICLES_SIZE | 3μm | |||||||
| MANUFACTURER | Imtakt | |||||||
| PRODUCT_NAME | Cadenza CD-C18 | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 10mM ammonium formate in ultrapure water; B = 0.1% formic acid in acetonitrile | ||||||
| LC_G_PROGRAM | B = 2% - 2 % (2 min) - 50 % (13min.) - 98 % (15 min) - 98 % (18 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.2 mL/min | |||||||
| MS Measurement condition | Ionization mode | negative | ||||||
| Desolvationtemperature | 270℃ | |||||||
| Needle voltage | 4000V | |||||||
| Velocity of Spectrum | 10 spec./sec. | |||||||
| Range of m/z | 155-2000 | |||||||
| Collision gas | He | |||||||
| TIC_JCAMP_FILE |  NIB-1178(-).jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
| ||||||||
| MEMO | sample: SHIGOKA (Eleutherococcus Senticosus Rhizome) water ext. 2 mg/mL (water/methanol 1:1) Injection Volume: 5μL シゴカ水抽出エキス 2 mg/mL （水/メタノール 1:1溶液） 注入量： 5μL | |||||||
| MS data list | ||||||||
| ||||||||
