Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameMAGNOLIAE FLOS
SampleNIB-1150
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH150mm
DIAMETER2.1mm
PARTICLES_SIZE2.6 μm
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% formic acid in ultrapure water; B = 0.1% formic acid in acetonitrile
LC_G_PROGRAMB = 2% - 2 % (5 min) - 98 % (30 min) - 98 % (35 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature270℃
Needle voltage4000V
Velocity of Spectrum10 spec./sec.
Range of m/z155-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-1150(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190-400
Memomeasured on a PDA
MEMOsample: SIN-I (Magnolia Flower) water ext. 2 mg/mL (water/methanol 1:1)
Injection Volume: 3μL

シンイ水抽出エキス 2 mg/mL (水/メタノール 1:1溶液)
注入量: 3μL
MS data list
Compound dataRetention time(min)MS data
Magnoflorine(マグノフロリン) 12.81 MS data