Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameMOUTAN CORTEX
SampleNIB-0268
CHROM_NAMEESI-Q-TOF(-)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH50mm
DIAMETER3.0mm
PARTICLES_SIZE2.6μm
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 0 - 70 % (30 min) – 100 % (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature450 ℃
Needle voltage-4,000 V
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0268_(-).jdx
3D(PDA) data
UV data
MEMOsample: BOTANPI (Moutan Bark) water ext. 1 mg/mL (water/methanol)
Injection Volume: 10μL

ボタンピ 水抽出エキス 1mg/mL (水/メタノール(1/1)溶液)
注入量: 10μL
MS data list