Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameAURANTII NOBILIS PERICARPIUM
SampleNIB-0665
CHROM_NAMEAPCI-Q-TOF(-)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH50mm
DIAMETER3.0mm
PARTICLES_SIZE2.6μm
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5 - 70 % (30 min) – 100 % (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature500 ℃
Needle voltage
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0665(-).jdx
3D(PDA) data
UV data
MEMOsample: CHINPI (Citrus Unshiu Peel) water ext. 1 mg/mL (water/methanol)
Injection Volume: 10 μL

チンピ 水抽出エキス 1mg/mL (水/メタノール(1/1)溶液)
注入量: 10 μL
MS data list
Compound dataRetention time(min)MS data
narirutin(ナリルチン) 14.068 MS data
Naringenin(ナリンゲニン) 20.921 MS data
Hesperidin(ヘスペリジン) 14.926 MS data