Crude drug latin name | SCUTELLARIAE RADIX |
Sample | NIB-0059 |
CHROM_NAME | ESI-Q-TOF(-) |
CHROM_TYPE | LC |
LC MACHINE TYPE | Agilent 1100 |
MS MACHINE TYPE | AB Sciex, QSTAR-XL |
Column | FILTER | ODS |
LENGTH | 150mm |
DIAMETER | 2.0mm |
PARTICLES_SIZE | 3um |
MANUFACTURER | KANTO CHEMICAL |
PRODUCT_NAME | Mightysil ODS |
LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile |
LC_G_PROGRAM | B = 5 - 70 % (30 min) – 100 % (35 min) |
COLUMN_TEMP | 40℃ |
FLOW_RATE | 0.2 mL/min |
MS Measurement condition | Ionization mode | negative |
Desolvationtemperature | 450 ℃ |
Needle voltage | -2,000 V |
Velocity of Spectrum | |
Range of m/z | 100-2000 |
Collision gas | N2, 35V |
TIC_JCAMP_FILE | NIB-0059(-).jdx |
3D(PDA) data | |
UV data |
MEMO | sample: OUGON (Scutellaria Root) ext. 0.2 mg/mL (water/methanol) |
MS data list |
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