LCMS data
Crude drug latin name | CINNAMOMI CORTEX | |
Sample | NIB-0014 | |
CHROM_NAME | APCI-Orbitrap(+) | |
CHROM_TYPE | LC | |
LC MACHINE TYPE | Shimadzu UFLC | |
MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap XL | |
Column | FILTER | ODS |
LENGTH | 150mm | |
DIAMETER | 4.6mm | |
PARTICLES_SIZE | 2.0μm | |
MANUFACTURER | GL science | |
PRODUCT_NAME | Inertsil ODS-4 | |
LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile |
LC_G_PROGRAM | B = 5 - 70 % (30 min) – 100 % (35 min) – 100 % (38 min) | |
COLUMN_TEMP | 40℃ | |
FLOW_RATE | 0.8 mL/min | |
MS Measurement condition | Ionization mode | positive |
Desolvationtemperature | 300 ℃ | |
Needle voltage | ||
Velocity of Spectrum | ||
Range of m/z | 100-2000 | |
Collision gas | He | |
TIC_JCAMP_FILE | NIB-0014(+).jdx | |
3D(PDA) data | ||
UV data | ||
MEMO | sample: KEIHI(Cinnamon Bark) water ext. 1 mg/mL (methanol) Injection Volume: 10μL(pos.), 30μL(neg.) ケイヒ 水抽出エキス 1 mg/mL (メタノール溶液) 注入量: 10μL(positiveモード), 30μL(negativeモード) | |
MS data list |