Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin namePERSICAE SEMEN
SampleNIB-0428
CHROM_NAMEESI-Q-TOF(+)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH150mm
DIAMETER2.0mm
PARTICLES_SIZE5μm
MANUFACTURERTosoh
PRODUCT_NAMETSK-gel ODS
LC Measurement conditionMOBILE_PHASEA = 10mM ammonium acetate and 0.02% acetic acid in ultrapure water; B = 10mM ammonium acetate and 0.02% acetic acid in acetonitrile
LC_G_PROGRAMB = 2 % - 70 % (30 min) – 100 % (35 min)- 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature450 ℃
Needle voltage+4,000 V
Velocity of Spectrum2 spectrum/sec.
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0428(+)TIC.jdx
3D(PDA) data
UV data
MEMOsample: TOUNIN (Peach Kernel) water ext. 1 mg/mL
Injection Volume: 10μL(pos.), 20μL(neg.)

トウニン 水抽出エキス 1 mg/mL
注入量: 10μL(positiveモード), 20μL(negativeモード)
MS data list