LCMS data
| Crude drug latin name | BUPLEURI RADIX | |||||||
| Sample | NIB-0190 | |||||||
| CHROM_NAME | ESI-Orbitrap(-) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | Shimadzu UFLC | |||||||
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap XL | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 100mm | |||||||
| DIAMETER | 2.1mm | |||||||
| PARTICLES_SIZE | 1.9μm | |||||||
| MANUFACTURER | ThermoScientific | |||||||
| PRODUCT_NAME | Hypersil GOLD | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile | ||||||
| LC_G_PROGRAM | B = 0 - 70 % (30 min) - 100 % (35 min) – 100 % (38 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.2 mL/min | |||||||
| MS Measurement condition | Ionization mode | negative | ||||||
| Desolvationtemperature | 300 ℃ | |||||||
| Needle voltage | -3000V | |||||||
| Velocity of Spectrum | 2 spectrum/sec. | |||||||
| Range of m/z | 100-2000 | |||||||
| Collision gas | He | |||||||
| TIC_JCAMP_FILE |  NIB-0190(-)TIC.jdx | |||||||
| 3D(PDA) data |  | |||||||
| UV data | ||||||||
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| MEMO | sample: SAIKO (Bupleurum Root) water ext. 1 mg/mL(water/methanol) Injection Volume: 10 μL サイコ 水抽出エキス 1mg/mL(水/メタノール溶液) 注入量：10 μL | |||||||
| MS data list | ||||||||
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