LCMS data
Crude drug latin name | ZINGIBERIS RHIZOMA | |||||||
Sample | NIB-0060 | |||||||
CHROM_NAME | ESI-Q-TOF(-) | |||||||
CHROM_TYPE | LC | |||||||
LC MACHINE TYPE | Agilent 1100 | |||||||
MS MACHINE TYPE | AB Sciex, QSTAR-XL | |||||||
Column | FILTER | ODS | ||||||
LENGTH | 150mm | |||||||
DIAMETER | 2.0mm | |||||||
PARTICLES_SIZE | 3μm | |||||||
MANUFACTURER | KANTO CHEMICAL | |||||||
PRODUCT_NAME | Mightysil ODS | |||||||
LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile | ||||||
LC_G_PROGRAM | B = 5 - 70 % (30 min) – 100 % (35 min) | |||||||
COLUMN_TEMP | 40℃ | |||||||
FLOW_RATE | 0.2 mL/min | |||||||
MS Measurement condition | Ionization mode | negative | ||||||
Desolvationtemperature | 450 ℃ | |||||||
Needle voltage | -2,000 V | |||||||
Velocity of Spectrum | ||||||||
Range of m/z | 100-2000 | |||||||
Collision gas | N2, 35V | |||||||
TIC_JCAMP_FILE | NIB-0060(-).jdx | |||||||
3D(PDA) data | ||||||||
UV data | ||||||||
MEMO | sample: SHOUKYOU (Ginger) water ext. 1 mg/mL (water/methanol) ショウキョウ 水抽出エキス 1 mg/mL (水/メタノール溶液) | |||||||
MS data list | ||||||||
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