LCMS data
| Crude drug latin name | ZINGIBERIS RHIZOMA | |||||||
| Sample | NIB-0169 | |||||||
| CHROM_NAME | ESI-Q-TOF(-) | |||||||
| CHROM_TYPE | LC | |||||||
| LC MACHINE TYPE | Agilent 1100 | |||||||
| MS MACHINE TYPE | AB Sciex, QSTAR-XL | |||||||
| Column | FILTER | ODS | ||||||
| LENGTH | 150mm | |||||||
| DIAMETER | 2.0mm | |||||||
| PARTICLES_SIZE | 3μm | |||||||
| MANUFACTURER | KANTO CHEMICAL | |||||||
| PRODUCT_NAME | Mightysil ODS | |||||||
| LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile | ||||||
| LC_G_PROGRAM | B = 5 - 70 % (30 min) – 100 % (35 min) | |||||||
| COLUMN_TEMP | 40℃ | |||||||
| FLOW_RATE | 0.2 mL/min | |||||||
| MS Measurement condition | Ionization mode | negative | ||||||
| Desolvationtemperature | 450 ℃ | |||||||
| Needle voltage | -2,000 V | |||||||
| Velocity of Spectrum | ||||||||
| Range of m/z | 100-2000 | |||||||
| Collision gas | N2, 35V | |||||||
| TIC_JCAMP_FILE |  NIB-0169(-).jdx | |||||||
| 3D(PDA) data | ||||||||
| UV data | ||||||||
| MEMO | sample: SHOUKYOU (Ginger) water ext. 1 mg/mL (water/methanol) ショウキョウ 水抽出エキス 1 mg/mL (水／メタノール溶液) | |||||||
| MS data list | ||||||||
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