Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameCNIDII RHIZOMA
SampleNIB-0048
CHROM_NAMEAPCI-Q-TOF(+)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH150mm
DIAMETER4.6mm
PARTICLES_SIZE5.0μm
MANUFACTURERTosoh
PRODUCT_NAMETSK-gel ODS
LC Measurement conditionMOBILE_PHASEA = 10mM ammonium acetate and 0.02% acetic acid in ultrapure water; B = 10mM ammonium acetate and 0.02% acetic acid in acetonitrile(containing 5% methanol)
LC_G_PROGRAMB = 5 - 70 % (30 min) - 100 % (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.8 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature
Needle voltage
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0048(+).jdx
3D(PDA) data
UV data
MEMOsample: SENKYUU (Cnidium Rhizome) water ext. 2 mg/mL
Injection Volume: 15 μL(pos.),10 μL(neg.)

センキュウ 水抽出エキス 2 mg/mL(水/アセトニトリル溶液)
注入量: 15 μL(positiveモード)、10 μL(negativeモード)
MS data list