Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameEVODIAE FRUCTUS
SampleNIB-0423
CHROM_NAMEESI-Q-TOF(+)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH150mm
DIAMETER2.0mm
PARTICLES_SIZE3um
MANUFACTURERImtakt
PRODUCT_NAMECadenza CD-C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5 - 60 % (30 min) - 100 % (35 min) - 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature500℃
Needle voltage+4500V
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0423(+).jdx
3D(PDA) data
UV data
MEMOsample: GOSHUYU (Euodia Fruit) water ext. 1 mg/mL (water/methanol)
After 1 minute ultrasonic irradiation and centrifuged, inject the supernatant liquid.
Injection Volume: 20 μL (pos.), 10 μL (neg.)

ゴシュユ 水抽出エキス 1 mg/mL (水/メタノール(1/1)溶液)
1分間超音波照射の後、遠心分離、上澄を注入。
注入量:20 μL(positiveモード)、10 μL(negativeモード)
MS data list