LCMS data
| Crude drug latin name | EVODIAE FRUCTUS | |
| Sample | NIB-0451 | |
| CHROM_NAME | ESI-Q-TOF(+) | |
| CHROM_TYPE | LC | |
| LC MACHINE TYPE | Agilent 1100 | |
| MS MACHINE TYPE | AB Sciex, QSTAR-XL | |
| Column | FILTER | ODS |
| LENGTH | 150mm | |
| DIAMETER | 2.0mm | |
| PARTICLES_SIZE | 3um | |
| MANUFACTURER | Imtakt | |
| PRODUCT_NAME | Cadenza CD-C18 | |
| LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile |
| LC_G_PROGRAM | B = 5 - 60 % (30 min) - 100 % (35 min) - 100 % (38 min) | |
| COLUMN_TEMP | 40℃ | |
| FLOW_RATE | 0.2 mL/min | |
| MS Measurement condition | Ionization mode | positive |
| Desolvationtemperature | 500℃ | |
| Needle voltage | +4500V | |
| Velocity of Spectrum | ||
| Range of m/z | 100-2000 | |
| Collision gas | N2, 35V | |
| TIC_JCAMP_FILE |  NIB-0451(+).jdx | |
| 3D(PDA) data | ||
| UV data | ||
| MEMO | sample: GOSHUYU (Euodia Fruit) water ext. 1 mg/mL (water/methanol) After 1 minute ultrasonic irradiation and centrifuged, inject the supernatant liquid. Injection Volume: 20 μL (pos.), 10 μL (neg.) ゴシュユ 水抽出エキス 1 mg/mL (水／メタノール（1/1）溶液) 1分間超音波照射の後、遠心分離、上澄を注入。 注入量：20 μL（positiveモード）、10 μL（negativeモード） | |
| MS data list | ||