Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameCINNAMOMI CORTEX
SampleNIB-0070
CHROM_NAMEAPCI-Orbitrap(-)
CHROM_TYPELC
LC MACHINE TYPEShimadzu UFLC
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap XL
ColumnFILTERODS
LENGTH150mm
DIAMETER4.6mm
PARTICLES_SIZE2.0μm
MANUFACTURERGL science
PRODUCT_NAMEInertsil ODS-4
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5 - 70 % (30 min) - 100 % (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.8 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature300 ℃
Needle voltage
Velocity of Spectrum
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0070(-).jdx
3D(PDA) data
UV data
MEMOsample: KEIHI(Cinnamon Bark) water ext. 1 mg/mL (methanol)
Injection Volume: 10μL(pos.), 30μL(neg.)

ケイヒ 水抽出エキス 1 mg/mL (メタノール溶液)
注入量: 10μL(positiveモード), 30μL(negativeモード)
MS data list