Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameUNCARIAE UNCIS CAM RAMLUS
SampleNIB-0465
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEShimadzu UFLC
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap XL
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE1.9μm
MANUFACTURERThermo Fisher Scientific
PRODUCT_NAMEHypersil GOLD C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 2% - 40 % (30 min) - 100 % (35 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature300 ℃
Needle voltage4000V
Velocity of Spectrum
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0465(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: CHOUTOUKOU (Uncaria Hook) water ext. 0.2 mg/mL (water/methanol)
Injection Volume: 10 μL

チョウトウコウ 水抽出エキス 0.2mg/mL (水/メタノール(1/1)溶液)
注入量: 10 μL
MS data list
Compound dataRetention time(min)MS data
Rhynchophylline(リンコフィリン) 20.12 MS data
Hirsutine(ヒルスチン) 24.93 MS data