Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameAURANTII NOBILIS PERICARPIUM
SampleNIB-0752
CHROM_NAMEESI-QqQ(+)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, API3000
ColumnFILTERODS
LENGTH50mm
DIAMETER3.0mm
PARTICLES_SIZE2.6um
MANUFACTURERPhenomenex
PRODUCT_NAMEKinetex C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5 - 70 % (30 min) - 100 % (35 min) - 100 % (38 min)
COLUMN_TEMP40 ℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature500 ℃
Needle voltage
Velocity of Spectrum
Range of m/z100-1000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0752(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190-400
Memomeasured on a DAD
MEMOsample: CHINPI (Citrus Unshiu Peel) water ext. 1 mg/mL
Injection Volume: 10 μL

チンピ 水抽出エキス 1mg/mL
注入量: 10 μL
MS data list
Compound dataRetention time(min)MS data
narirutin(ナリルチン) 11.240 MS data
Hesperidin(ヘスペリジン) 11.960 MS data
Nobiletin(ノビレチン) 21.022 MS data