Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameOPHIOPOGONIS TUBER
SampleNIB-0390
CHROM_NAMEESI-Q-TOF(+)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH150mm
DIAMETER2.0mm
PARTICLES_SIZE3μm
MANUFACTURERImtakt
PRODUCT_NAMECadenza CD-C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 8 - 70 % (30 min) - 100 % (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature450 ℃
Needle voltage+5000V
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0390(+).jdx
3D(PDA) data
UV data
MEMOsample: BAKUMONDOU (Ophiopogon Root) water ext. 4 mg/mL (water/methanol)
Injection Volume: 10μL(pos.), 15μL(neg.)

バクモンドウ 水抽出エキス 4 mg/mL (水/メタノール溶液)
注入量: 10μL(positiveモード), 15μL(negativeモード)
MS data list