LCMS data
| Crude drug latin name | OPHIOPOGONIS TUBER | |
| Sample | NIB-0392 | |
| CHROM_NAME | ESI-Q-TOF(-) | |
| CHROM_TYPE | LC | |
| LC MACHINE TYPE | Agilent 1100 | |
| MS MACHINE TYPE | AB Sciex, QSTAR-XL | |
| Column | FILTER | ODS |
| LENGTH | 150mm | |
| DIAMETER | 2.0mm | |
| PARTICLES_SIZE | 3μm | |
| MANUFACTURER | Imtakt | |
| PRODUCT_NAME | Cadenza CD-C18 | |
| LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile |
| LC_G_PROGRAM | B = 8 - 70 % (30 min) - 100 % (35 min) – 100 % (38 min) | |
| COLUMN_TEMP | 40℃ | |
| FLOW_RATE | 0.2 mL/min | |
| MS Measurement condition | Ionization mode | negative |
| Desolvationtemperature | 450 ℃ | |
| Needle voltage | -4000V | |
| Velocity of Spectrum | ||
| Range of m/z | 100-2000 | |
| Collision gas | N2, 35V | |
| TIC_JCAMP_FILE |  NIB-0392(-).jdx | |
| 3D(PDA) data | ||
| UV data | ||
| MEMO | sample: BAKUMONDOU (Ophiopogon Root) water ext. 4 mg/mL (water/methanol) Injection Volume: 10μL(pos.), 15μL(neg.) バクモンドウ 水抽出エキス 4 mg/mL (水/メタノール溶液) 注入量： 10μL(positiveモード), 15μL(negativeモード) | |
| MS data list | ||