Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameCOPTIDIS RHIZOMA
SampleNIB-0013
CHROM_NAMEESI-Q-TOF(+)
CHROM_TYPELC
LC MACHINE TYPEAgilent 1100
MS MACHINE TYPEAB Sciex, QSTAR-XL
ColumnFILTERODS
LENGTH150mm
DIAMETER2.0mm
PARTICLES_SIZE3um
MANUFACTURERKANTO CHEMICAL
PRODUCT_NAMEMightysil ODS
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5 - 70 % (30 min.) - 100 % (35 min.)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature450 ℃
Needle voltage+5,000 V
Velocity of Spectrum
Range of m/z100-2000
Collision gasN2, 35V
TIC_JCAMP_FILE
NIB-0013(+).jdx
3D(PDA) data
UV data
MEMOsample: OUREN (Coptis Rhizome) water ext. 1 mg/mL (water)

オウレン 水抽出エキス 1mg/mL(水溶液)
MS data list
Compound dataRetention time(min)MS data
Berberine (ベルベリン) 15.394 MS data
Coptisine (コプチシン) 14.059 MS data
Palmatine (パルマチン) 15.518 MS data