Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin name ASTRAGALI RADIX
Sample NIB-0415
CHROM_NAME ESI-Orbitrap(+)
CHROM_TYPE LC
LC MACHINE TYPE ThermoFisher Scientific Ultimate 3000
MS MACHINE TYPE ThermoFisher Scientific LTQ Orbitrap Elite
Column FILTER ODS
LENGTH 100 mm
DIAMETER 2.1mm
PARTICLES_SIZE 2.2 um
MANUFACTURER Thermo Scientific
PRODUCT_NAME Acclaim RSLC 120 C18
LC Measurement condition MOBILE_PHASE A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAM B = 5 % (0 min) - 70 % (30 min) - 100 % (35 min) - 100 % (38 min)
COLUMN_TEMP 40℃
FLOW_RATE 0.2 mL/min
MS Measurement condition Ionization mode positive
Desolvationtemperature 450 ℃
Needle voltage 3000 V
Velocity of Spectrum 10 spec./sec.
Range of m/z 100-2000
Collision gas He
TIC_JCAMP_FILE
NIB-0415(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm) 190 – 800
Memo measured on a PDA
MEMO sample: OUGI (Astragalus Root) water ext. 2 mg/mL (methanol:water = 1:1)
Injection Volume: 15 μL

オウギ 水抽出エキス 2 mg/mL(メタノール:水　1:1　溶液)
注入量：15 μL
MS data list
Compound data Retention time(min) MS data
Calycosin 7-O-Glucoside (カリコシン7-O-グルコシド) 11.52 MS data