Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameASTRAGALI RADIX
SampleNIB-0299
CHROM_NAMEESI-Orbitrap(-)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100 mm
DIAMETER2.1 mm
PARTICLES_SIZE2.2 um
MANUFACTURERThermo Scientific
PRODUCT_NAMEAcclaim RSLC 120 C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5 % (0 min) - 70 % (30 min) - 100 % (35 min) - 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature450 ℃
Needle voltage- 3000 V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0299(-).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: OUGI (Astragalus Root) water ext. 2 mg/mL (methanol:water = 1:1)
Injection Volume: 15 μL

オウギ 水抽出エキス 2 mg/mL(メタノール:水 1:1 溶液)
注入量:15 μL
MS data list
Compound dataRetention time(min)MS data
Astragaloside Ⅳ(アストラガロシドⅣ) 20.64 MS data
Calycosin 7-O-Glucoside (カリコシン7-O-グルコシド) 11.53 MS data