Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameARMENIACAE SEMEN
SampleNIB-0425
CHROM_NAMEESI-Orbitrap(-)
CHROM_TYPELC
LC MACHINE TYPEShimadzu UFLC
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap XL
ColumnFILTERODS
LENGTH100 mm
DIAMETER2.1 mm
PARTICLES_SIZE1.9 um
MANUFACTURERThermo Scientific
PRODUCT_NAMEHypersil GOLD
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 2 - 20 % (5 min) - 60% (30 min)- 90% (35 min) – 100 % (38 min)
COLUMN_TEMP40℃
FLOW_RATE0.2 mL/min
MS Measurement conditionIonization modenegative
Desolvationtemperature300 ℃
Needle voltage4000 V
Velocity of Spectrum
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0425(-).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: KYOUNIN (Apricot Kernel) water ext. 1 mg/mL (water:methanol = 1:1)
injection vol. = 10 uL

キョウニン 水抽出エキス 1 mg/mL (水/メタノール(1:1)溶液)
注入量 : 10uL
MS data list
Compound dataRetention time(min)MS data
Amygdalin(アミグダリン) 9.69 MS data