LCMS data
Crude drug latin name | SCHISANDRAE FRUITS | ||||||||||
Sample | NIB-0437 | ||||||||||
CHROM_NAME | ESI-Orbitrap(+) | ||||||||||
CHROM_TYPE | LC | ||||||||||
LC MACHINE TYPE | ThermoFisher Scientific Ultimate 3000 | ||||||||||
MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap Elite | ||||||||||
Column | FILTER | ODS | |||||||||
LENGTH | 100mm | ||||||||||
DIAMETER | 2.1mm | ||||||||||
PARTICLES_SIZE | 2.6μm | ||||||||||
MANUFACTURER | ChromaNik Technologies | ||||||||||
PRODUCT_NAME | SunShell C18 | ||||||||||
LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile | |||||||||
LC_G_PROGRAM | B = 5% - 100 % (15 min) - 100 % (17 min) | ||||||||||
COLUMN_TEMP | 40℃ | ||||||||||
FLOW_RATE | 0.25 mL/min | ||||||||||
MS Measurement condition | Ionization mode | positive | |||||||||
Desolvationtemperature | 450 ℃ | ||||||||||
Needle voltage | 3000V | ||||||||||
Velocity of Spectrum | 10 spec./sec. | ||||||||||
Range of m/z | 100-2000 | ||||||||||
Collision gas | He | ||||||||||
TIC_JCAMP_FILE | NIB-0437(+).jdx | ||||||||||
3D(PDA) data | |||||||||||
UV data | |||||||||||
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MEMO | sample: GOMISHI (Schisandra Fruit) water ext. 0.2 mg/mL (water/methanol = 1:1) Injection Volume: 3 μL ゴミシ 水抽出エキス 0.2mg/mL (水/メタノール(1/1)溶液) 注入量: 3 μL | ||||||||||
MS data list | |||||||||||
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