Comprehensive Medicinal Plant Database

LCMS data

Crude drug latin nameSCHISANDRAE FRUITS
SampleNIB-0737
CHROM_NAMEESI-Orbitrap(+)
CHROM_TYPELC
LC MACHINE TYPEThermoFisher Scientific Ultimate 3000
MS MACHINE TYPEThermoFisher Scientific LTQ Orbitrap Elite
ColumnFILTERODS
LENGTH100mm
DIAMETER2.1mm
PARTICLES_SIZE2.6μm
MANUFACTURERChromaNik Technologies
PRODUCT_NAMESunShell C18
LC Measurement conditionMOBILE_PHASEA = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile
LC_G_PROGRAMB = 5% - 100 % (15 min) - 100 % (17 min)
COLUMN_TEMP40℃
FLOW_RATE0.25 mL/min
MS Measurement conditionIonization modepositive
Desolvationtemperature450 ℃
Needle voltage3000V
Velocity of Spectrum10 spec./sec.
Range of m/z100-2000
Collision gasHe
TIC_JCAMP_FILE
NIB-0737(+).jdx
3D(PDA) data
UV data
UV chromatogram
Wavelength(nm)190 – 800
Memomeasured on a PDA
MEMOsample: GOMISHI (Schisandra Fruit) water ext. 0.2 mg/mL (water/methanol = 1:1)
Injection Volume: 3 μL

ゴミシ 水抽出エキス 0.2mg/mL (水/メタノール(1/1)溶液)
注入量: 3 μL
MS data list
Compound dataRetention time(min)MS data
Schizandrin(シザンドリン) 9.91 MS data
Gomisin A(ゴミシンA) 10.48 MS data