| Crude drug latin name
| PHELLODENDRI CORTEX |
| Sample
| |
| NMR type
| 13C-NMR |
| Machine
| JEOL ECA600 |
| Magnetic field (MHz)
| 600.17 MHz |
| Solvent
| CD3OD |
| Mesurement temperature (deg)
| 21.300 |
| Number of excitations (times)
| 10000 |
| Sample weight
| |
| spectrum
|  |
| Jcamp file
| palmatine chloride_CARBON-1.jdx (viewer *for windows) |
| FID file
| palmatine chloride_CARBON-1.jdf |
| Assignment
|
| Assign
|
Peak(ppm)
|
| 2 |
27.81 |
| 1 |
56.68 |
| (-O-CH3) |
57.00 |
| (-O-CH3) |
57.36 |
| (-O-CH3) |
57.66 |
| (-O-CH3) |
62.53 |
| 18 |
109.97 |
| 15 |
112.23 |
| 12 |
120.50 |
| 6 |
121.29 |
| 4 |
123.31 |
| 9 |
124.45 |
| 8 |
128.09 |
| 3 |
130.09 |
| 7 |
135.31 |
| 5 |
139.86 |
| 10 |
145.78 |
| 13 |
146.42 |
| 17 |
150.95 |
| 16 |
151.93 |
| 11 |
153.86 |
|
| Compound name
|
Palmatine Chloride（パルマチン塩化物）
|
| Memo
| リファレンスは溶媒に合わせて測定
assignment reference: Min, Yong Deuk; Archives of Pharmacal Research 2006, V29(9), P757-761 |