| Crude drug latin name
| GARDENIAE FRUCTUS |
| Sample
| |
| NMR type
| 1H-NMR |
| Machine
| JEOL ECA600 |
| Magnetic field (MHz)
| 600.17 MHz |
| Solvent
| CD3OD |
| Mesurement temperature (deg)
| 21.000 |
| Number of excitations (times)
| 16 |
| Sample weight
| |
| spectrum
|  |
| Jcamp file
| geniposide_PROTON-1.jdx (viewer *for windows) |
| FID file
| geniposide_PROTON-1.jdf |
| Assignment
|
| Assign
|
Peak(ppm)
|
Integral
|
| 6 |
2.08 |
1.05 |
| 9 |
2.71 |
1.06 |
| 6 |
2.81 |
1.05 |
| 5 |
3.17 |
0.95 |
| 2', 3', 4', 5' |
3.19-3.38 |
|
| 6' |
3.62 |
1.05 |
| 12 |
3.70 |
3.02 |
| 6' |
3.84 |
1.03 |
| 10 |
4.17 |
1.02 |
| 10 |
4.30 |
1.02 |
| 1' |
4.69 |
1.03 |
| 1 |
5.16 |
1.00 |
| 7 |
5.78 |
1.00 |
| 3 |
7.5 |
0.95 |
|
| Compound name
|
Geniposide（ゲニポシド）
|
| Memo
| リファレンスは溶媒に合わせて測定
assignment reference: Guvenalp, Zuhal; Turkish Journal of Chemistry 2006, V30(4), P515-523 |